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KMID : 0385520120250060410
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Analytical Science & Technology
2012 Volume.25 No. 6 p.410 ~ p.415
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Fundamental study on the development of the testing method of Triclosan with GC/ECD and GC/MS
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Jeong Hui-Jae
Lee Jae-In
Kweon Deok-Jun
Eom Hui-Jeong
Choi Zel-Ho
Chio Ki-In
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Abstract
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In this study, a fundamental study was conducted to establish the method for quantitative analysis and pretreatment of triclosan, one of the chemicals to be used as bactericides, detergents, and sterilizers. The extraction efficiency of triclosan was the highest when it was extracted by soxhlet apparatus with n-hexane, and it showed a satisfactory result when the samples were analyzed with both GC/ECD and GC/MS. To evaluate the reproductivity of the results, each 30 reference samples made with paper filter and cotton wool was prepared in this study. From the results with high extraction effectiveness, low analysis deviation, and good statistical analysis data, the method for the extraction and analysis for triclosan were resonable for the paper and textile samples applied in this study.
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KEYWORD
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Triclosan, GC-MS, GC-ECD, test method
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